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Beilstein J. Org. Chem. 2018, 14, 2425–2434, doi:10.3762/bjoc.14.220
Graphical Abstract
Figure 1: Selected homogeneous catalysts for alkyne metathesis.
Scheme 1: Synthesis of alkylidyne complex V from bimetallic [(t-BuO)3W≡W(Ot-Bu)3]; the catalytically active d...
Scheme 2: Synthesis of hexakis(fluoroalkoxide) dimers Mo2F6 [73] and W2F3.
Figure 2: Molecular structure of W2F3·NHMe2 with thermal displacement parameters drawn at 50% probability. Hy...
Scheme 3: Preparation of the alkylidyne complex WPhF3.
Figure 3: Molecular structure of WPhF3 with thermal displacement parameters drawn at 50% probability. Hydroge...
Scheme 4: Self-metathesis of 1-phenyl-1-propyne derivatives by tungsten complexes W2F3 and WPhF3.
Figure 4: Conversion versus time diagram for the self-metathesis of 1-phenyl-1-propyne catalyzed by 0.5 mol % ...